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2,4-Bis(2,4-dimethoxyphenyl)-1,3-dithia-2,4-diphosphetane 2,4-disulfide and its derivatives: Syntheses, structural characterizations, anticancer activities, and theoretical studies on some dithiophosphonato Ni(II) complex

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dc.creator Zorlu, Yunus
dc.creator Yılmaz, Hamza
dc.creator Zeyrek, Celal Tuğrul
dc.creator Bulat, Elif
dc.creator SAĞLAM, ERTUĞRUL GAZİ
dc.creator AKKOÇ, Senem
dc.date 2023-01-15T00:00:00Z
dc.date.accessioned 2025-02-25T10:41:21Z
dc.date.available 2025-02-25T10:41:21Z
dc.identifier f1331fd3-c83e-46a1-bba6-a42220ad0b00
dc.identifier 10.1016/j.molstruc.2022.134197
dc.identifier https://avesis.sdu.edu.tr/publication/details/f1331fd3-c83e-46a1-bba6-a42220ad0b00/oai
dc.identifier.uri http://acikerisim.sdu.edu.tr/xmlui/handle/123456789/101887
dc.description © 2022New 2,4-bis(2,4-dimethoxyphenyl)-1,3-dithia-2,4-diphosphetane 2,4-disulfide, (SAV-A2), was synthesized from the reaction P4S10 and 1,3-dimethoxybenzene. SAV-A2 was reacted with alcohols to form dithiophosphonic acid monoesters (HLn, HS2P((2,4-CH3O)2C6H3)(ORn); n=1–3, R1=2‑butyl‑; R2=n-pentyl-; R3=4‑tert‑but-benzyl-). The acids were converted to the ammonium salts ([NH4Ln]) to serve as the source of the ligands (Ln), to obtain Ni(II) complexes, ([Ni(Ln)2]). [Ni(L2)2] crystal structure was elucidated by single-crystal X-ray diffraction analysis. In addition, Density Functional Theory (DFT) calculations of [Ni(L2)2] was performed. The molecular docking studies of the complex with liver cancer protein, PDB ID: 3WZE and colon cancer antigen proteins, ID 2HQ6 were done compare with experimental and theoretical results. All compounds were tested on liver- and colon cancer cell lines. Among the complexes tested, [Ni(L3)2] showed an activity closer to that of cisplatin against the colon cancer cell line. The other compounds were found to be have less active.
dc.language eng
dc.rights info:eu-repo/semantics/closedAccess
dc.title 2,4-Bis(2,4-dimethoxyphenyl)-1,3-dithia-2,4-diphosphetane 2,4-disulfide and its derivatives: Syntheses, structural characterizations, anticancer activities, and theoretical studies on some dithiophosphonato Ni(II) complex
dc.type info:eu-repo/semantics/article


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