| dc.creator |
Karahan, Ahmet |
|
| dc.creator |
Yardan, Alper |
|
| dc.creator |
Yahşi, Yasemin |
|
| dc.creator |
Kara, Hülya |
|
| dc.creator |
Kurtaran, Raif |
|
| dc.date |
2013-04-16T00:00:00Z |
|
| dc.date.accessioned |
2019-07-09T11:48:47Z |
|
| dc.date.available |
2019-07-09T11:48:47Z |
|
| dc.identifier |
http://dergipark.org.tr/sdufeffd/issue/11278/134751 |
|
| dc.identifier |
|
|
| dc.identifier.uri |
http://acikerisim.sdu.edu.tr/xmlui/handle/123456789/45809 |
|
| dc.description |
Cu(II) kompleksinin X-ışınları moleküler yapısı 293 K'de tayin edildi. Cu (II) kompleksi monoklinik yapıda ve uzay grubu P21/n a= 12.4007(14), b= 8.4476(9), c= 20.0286(12) Ã…, β= 97.291(7)°. Termal davranışları diferansiyel termal analiz ve termogravimetrik analiz ile incelendi. Ayrıca Schiff bazı ligandının karakterizasyonunda elementel analiz, IR, UV-vis spektroskopisi, termal analiz, 1H-NMR ve 13C-NMR yöntemlerinden faydalanıldı. Anahtar kelimeler: Schiff bazı, Tek Kristal, X-ışınları analizi, Termal analizThe X-Ray Molecular Structure and Thermal Behaviour of Cu (II) Complex, Synthesis With N2O2 Type Schiff Base Ligand Abstract: The X-ray molecular structure of Cu (II) complex at 293 K has been determined. The Cu (II) complex, has been prepared and structurally and thermal characterized. The complex crystallizes in monoclinic space group P21/n with a= 12.407(14), b= 8.4476(9), c= 20.0286(12) Ã…, β= 97.291(7)°. The thermal behavior of the compound was investigated by differential thermal analysis and thermogravimetry. Additionally, Schiff base ligand also characterized by elemental analysis, IR, UV-vis spectroscopy, thermal analysis, 1H-NMR and 13C-NMR. Key words: Schiff base, Single crystal, X-ray analysis, Thermal analysis |
|
| dc.description |
The X-ray molecular structure of Cu (II) complex at 293 K has been determined. The Cu (II) complex, has been prepared and structurally and thermal characterized. The complex crystallizes in monoclinic space group P21/n with a= 12.407(14), b= 8.4476(9), c= 20.0286(12) Å, β= 97.291(7)°. The thermal behavior of the compound was investigated by differential thermal analysis and thermogravimetry. Additionally, Schiff base ligand also characterized by elemental analysis, IR, UV-vis spectroscopy, thermal analysis, 1H-NMR and 13C-NMR |
|
| dc.format |
application/pdf |
|
| dc.language |
tr |
|
| dc.publisher |
Süleyman Demirel University |
|
| dc.publisher |
Süleyman Demirel Üniversitesi |
|
| dc.relation |
http://dergipark.org.tr/download/article-file/116365 |
|
| dc.source |
Volume: 8, Issue: 2
163-174 |
en-US |
| dc.source |
1306-7575 |
|
| dc.subject |
Schiff bazı, Tek Kristal, X-ışınları analizi, Termal analiz |
|
| dc.subject |
Schiff base, Single crystal, X-ray analysis, Thermal analysis |
|
| dc.title |
N2O2 Tipi Schiff Bazı Ligandı ile Sentezlenen Cu(II) Kompleksinin X-Işını Yapısı ve Termal Özelliği |
en-US |
| dc.type |
info:eu-repo/semantics/article |
|